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SAXS2 Beamline
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The SAXS2 beamline is an experimental station dedicated to Small Angle X-ray Scattering (SAXS) techniques in the hard x-rays energy range (6 to 12 keV) for studying the shape, size and structures of soft materials in the nanoscale with sizes ranging from 1 to 100 nm, with applications to molecular biology, medicine, life science, chemistry and material science.

CONTACT & STAFF

For more information on this beamline, contact us.

EXPERIMENTAL TECHNIQUES

The following experimental techniques and setups are available to users in this beamline. To learn more about the techniques’ limitations and requirements (sample, environment, etc.) contact the beamline coordinator before submitting your proposal.

  • SMALL ANGLE X-RAY SCATTERING (SAXS)
  • WIDE ANGLE X-RAY SCATTERING (WAXS)

LAYOUT & OPTICAL ELEMENTS

ElementTypePosition [m]Description
SOURCEBending Magnet0.0Bending Magnet D02 exit A (4°), 1.67 T
M1Vertical Focusing Mirror6.3
MONOSide Bounce Monochromator8.8Si(111) - 11°
ESExperimental Station14.0

PARAMETERS

ParameterValueCondition
Energy range [keV]6-12Si(111)
Energy Resolution [$ \Delta$E/E]0.1

INSTRUMENTATION

InstrumentTypeModelManufacturerSpecifications
CCD DetectorAreaCCD-Mar165--
Furnace--Temp.: 25°C - 1200°C LNLS in-house development
Capillary--Room TemperatureLNLS in-house development
PASMI--Temp.: 25°C - 90°CLNLS in-house development
PALMI--Temp.: 25°C - 90°CLNLS in-house development
PALMIMLiquid cell with magnetic field -0 T – 1.2 T; Temp.: 25°C - 95°CLNLS in-house development
LinkamDSC600---

CONTROL AND DATA ACQUISITION

All beamline controls are done through EPICS (Experimental Physics and Industrial Control System), running on a PXI from National Instruments. The data acquisition is done using a Red Hat workstation with the Py4Syn, developed at LNLS by SOL group.

All equipment has been synchronized through PXI to render the experiments easy and simple as possible. Long temperature scans with different furnaces are atomized and easy to performed.

HOW TO CITE THIS FACILITY

Users are required to acknowledge the use of LNLS facilities in any publications and to inform the Laboratory about any publications, thesis and other published materials. Users must also cooperate by supplying this information upon request. 

Support text for acknowledgements:

This research used resources of the Brazilian Synchrotron Light Laboratory (LNLS), an open national facility operated by the Brazilian Centre for Research in Energy and Materials (CNPEM) for the Brazilian Ministry for Science, Technology and Innovations (MCTI). The _ _ _ beamline staff is acknowledged for the assistance during the experiments.

PUBLICATIONS

Scientific publications produced with data obtained at the facilities of this beamline, and published in journals indexed by the Web of Science, are listed below.

Attention Users: Given the importance of the previous scientific results to the overall proposal evaluation process, users are strongly advised to check and update their publication record both at the SAU Online website and at the CNPEM library database. For the library, updates can be made by sending the full bibliographic data to the CNPEM library (biblioteca@cnpem.br). Publications are included in the database after being checked by the CNPEM librarians and the beamline coordinators.

Martins, F. H.; Paula, F. L. O.; Gomes, R. C.; Gomes, J. A.; Aquino, R.; Porcher, F.; Perzynski, R.; Depeyrot, J.. Local Structure Investigation of Core-Shell CoFe2O4@gamma-Fe2O3 Nanoparticles, Brazilian Journal of Physics, v.51, p. 47–59, 2021. DOI:10.1007/s13538-020-00829-9

Silva, L. F. da; Catto, A. C.; Bernardini, S.; Fiorido, T.; Palma, J. V. N. de ; Avansi Jr., W.; Aguir, K.; Bendahan, M.. BTEX gas sensor based on hematite microrhombuses, Sensors and Actuators B-Chemical, v. 326, p. 128817, 2020. DOI:10.1016/j.snb.2020.128817

Pereira, M. O.; Felix, V. de S. ; Oliveira-Carvalho, A. L.; Ferreira, D. S. R.; PImenta, A. R. ; Carvalho, C. S.; Silva, F. L. e; Pérez, C. A.; Galante, D.; Freitas, R. P. de. Investigating counterfeiting of an artwork by XRF, SEM-EDS, FTIR and synchrotron radiation induced MA-XRF at LNLS-BRAZIL, Spectrochimica Acta Part A-Molecular and Biomolecular Spectroscopy, v. 246, p. 118925, 2021. DOI:10.1016/j.saa.2020.118925

Lopes, N. A. ; Mertins, O.; Pinilla, C. M. B. ; Brandelli, A.. Nisin induces lamellar to cubic liquid-crystalline transition in pectin and polygalacturonic acid liposomes, Food Hydrocolloids, v. 112, p.106320, 2021. DOI:10.1016/j.foodhyd.2020.106320

Coura, R, L. C. ; Andrade, A. B.; Monteiro, T. de J.; Novais, S. M. V.; Macedo, Z. S.; Valerio, M. E. G.. Photoluminescent properties of BaF2 scintillator-polystyrene composite films under vacuum ultraviolet radiation, Materials Research Bulletin, v.135, p. 111159, 2021. DOI:10.1016/j.materresbull.2020.111159

Moreno, H.; Cortes, J. A. ; Praxedes, F. M. ; Freitas, S. M. de; Rezende, M. V. dos S.; Simões, A. Z. ; Teixeira, V. C.; Ramírez, M. A.. Tunable photoluminescence of CaCu3Ti4O12 based ceramics modified with tungsten, Journal of Alloys and Compounds, v.850, p. 156652, 2021. DOI:10.1016/j.jallcom.2020.156652

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